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气-质联机对嗪草酮原药及其主要杂质的分析
GC-MS analysis of metribuzin technical and its main impurities

气-质联机对嗪草酮原药及其主要杂质的分析

ISSN:1006-0413
2006年第45卷第9期
农药分析
刘伟[1],吴文君[2] LIU Wei[1],WU Wen-jun[2]
  1. 农业部农药质量监督检验测试中心,西安,710003
  2. 西北农林科技大学,陕西,杨凌,712100

采用气桐色谱-质谱(GC—MS)联用对嗪草酮原药主成分及主要杂质进行分析,结合嗪草酮原药合成工艺,确定了3个主要杂质的结构和含量。同时利用杂质结构对嗪草酮的合成新方法进行验证。


Gas chromatography-mass spectroscopy analysis was conducted on the primary ingredient of metribuzin technical as well as its primary impurities, in conjunction with metribuzin synthesis methodology. The structures and contents of three main impurities of metrihuzin were identified, and these structures were used in validating a new method of metribuzin synthesis.

关键词: 嗪草酮气-质联用杂质合成方法
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ISSN:1006-0413
2006年第45卷第9期
农药分析

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