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An efficient one-pot synthesis of annulated pyridines utilising a directed ortho-metallation/transmetallation approach

ISSN:0040-4039
2004年第45卷第8期
Antony J. Davies:tony_davies2@merck.com,Karel M.J. Brands,Cameron J. Cowden,Ulf-H. Dolling,David R. Lieberman

The ortho-alkylation of Boc-protected aminopyridines with α,ω-dihaloalkanes followed by in situ cyclisation, resulted in the corresponding annulated pyridine derivatives in good to excellent yields. The effect of the alkylating and chelating agents, the transmetallation additives and the directing group was examined.

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ISSN:0040-4039
2004年第45卷第8期

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