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PVP保护下纳米银颗粒的液相化学还原法制备及表征

PVP保护下纳米银颗粒的液相化学还原法制备及表征

ISSN:1004-0676
2014年第35卷第4期
王春霞[1]    李英琳[1]    徐磊[2] WANG Chunxia[1] , LI Yinglin[1] , XU Lei[2]

以PVP为表面活性剂,甲酸铵为还原剂,采用液相还原法制备了纳米银颗粒。采用X射线衍射(XRD)、透射电子显微镜(TEM)和紫外-可见光吸收光谱(UV-Vis)对所制备样品进行表征。结果显示:当PVP与AgNO3的质量比为2.2:1,陈化时间24 h,得到立方块和六棱柱的银混合颗粒。

Nano-silver particles were prepared by using polyvinyl pyrolidone as the dispersing agent and ammonium as the reducing agent. The resulting specimens were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM) and UV-Vis adsorption spectrum. The result revealed that a mixture of cube and hexagonal prisms of nano-silver particles was obtained when the mass ratio of PVP to AgNO3 was 2.2:1 and the aging time was 24 hours.

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ISSN:1004-0676
2014年第35卷第4期

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